|
|
Introduction:
|
1
|
Theoretical
background - polymer synthesis |
2
|
Theoretical background - liquid
chromatography |
3
|
Comparison and differentiation
between GPC/SEC and
HPLC |
4
|
Objectives of GPC/SEC Analysis
|
|
Fundamentals:
|
5
|
GPC/SEC Separation mechanism |
6
|
Retention, plate count, resolution,
efficiency |
7
|
Molar mass determination |
8
|
Molar mass distribution: averages,
moments, meaning |
|
Experimental Setup and
Parameters: |
9
|
GPC/SEC instruments and systems |
| 10 |
Column selection and method optimization |
11
|
Increasing accuracy and reproducibility |
12
|
Influence
analytical
conditions |
|
GPC/SEC Calibration Methods:
|
13
|
Calibration
with molar mass standards
|
14
|
Universal
Calibration
|
15
|
Broad
Calibration
|
16
|
Integral
Calibration
|
17
|
Copolymer
calibration options
|
18
|
Molar
mass determination with viscometer and/or light
scattering detection
|
|
Modern Copolymer Analysis using GPC/SEC
|
19
|
Definition
and analytical problems copolymers
|
20
|
Dual
detection for copolymer composition analysis
|
21
|
On-line
viscometry and coupling with FTIR-Detection
|
22
|
2-dimensional
chromatography
|
